AQUASOMIC

Results


Documents and data handle are stored in non-propietary data formats in public data repositories such as own institutional repositories and Zenodo. 

Validated target and efficient nontarget methods of analysis of emerging contaminants in surface waters and biofluids 


Mikel Musatadi, Iker Alvarez-Mora, Ines Baciero-Hernandez, Ailette Prieto, Eneritz Anakabe, Maitane Olivares, Nestor Etxebarria, Olatz Zuloaga, Sample preparation for suspect screening of persistent, mobile and toxic substances and their phase II metabolites in human urine by mixed-mode liquid chromatography, Talanta 271, 125698 (2024)
Mikel Musatadi, Inés Baciero-Hernández, Ailette Prieto, Maitane Olivares, Nestor Etxebarria, Olatz Zuloaga, Development and evaluation of a comprehensive workflow for suspect screening of expsome-related xenobiotics and phase II metabolites in diverse human biofluids, Chemosphere 351, 141221 (2024) 
I. Baciero-Hernández, M. Musatadi, M. Olivares, A. Prieto, N. Etxebarria, O. Zuloaga, Sample preparation for suspect and non-target screening of xenobiotics in human biofluids by liquid chromatography-high resolution tandem mass spectrometry, MethodsX 12, 102501 (2024) 
Sara Fernandes, Andreia Meireles, Sara Marques, Luis Silva, Luisa Barreiros, Benedita Sampaio-Maia, Manuel Miró, Marcela A. Segundo, Sample preparation and chromatographic methods for the determination of protein-bound uremic retention solutes in human biological samples: an overview, Journal Chromatography B, 1215, 123578 (2023)
Mikel Musatadi, Asier Andrés-Maguregi, Francesca De Angelis, Ailette Prieto, Eneritz Anakabe, Maitane Olivares, Nestor Etxebarria, Olatz Zuloaga, The role of sample preparation in suspect and non-target screening for exposome analysis using human urine, Chemosphere 339, 139690 (2023) 
Mikel Musatadi, Jon Zumalabe, Leire Mijangos, Ailette Prieto, Maitane Olivares, Olatz Zuloaga, Dilute-and-shoot coupled to mixed mode liquid chromatography-tandem mass spectrometry for the analysis of persistent and mobile organic compounds in human urine, Journal of Chromatography A 1705, 464141 (2023) 
Leire Mijangos, Dennis Bilbao, Naroa Lopez-Herguedas, Olatz Zuloaga, Nestor Etxebarria, Ailette Prieto, Development of an analytical method for the simultaneous determination of 50 semi-volatile organic contaminants in wastewaters. MethodsX 11,  102252 (2023)
N. Fontanals, E. Pocurull, R. Montes, I. Gonzalez-Mariño, S. Santana-Viera, M. Miró, A. Rico, S. Rodríguez-Mozaz, F. Borrull, J.B. Quintana, R.M. Marcé, A new analytical method to determine trace level concentrations of pharmaceuticals in influent wastewater: A tool to monitor human use patterns, Microchem J 193, 109131 (2023)
Hernández F., Fabregat-Safon D., Campos-Maña M., Quintana J.B. Efficient Validation Strategies in Environmental Analytical Chemistry: A Focus on Organic Micropollutants in Water Samples Annual Review of Analytical Chemistry, 16, 401 - 428 (2023)
Carro N., Fernández R., Sóñora S., Cobas J., García I., Ignacio M., Mouteira A.Optimization of micro-QuEChERS extraction coupled with gas chromatography-mass spectrometry for the fast determination of phthalic acid esters in mussel samples, Analytical Methods, 15 (14), 1836 - 1845 (2023)
Musatadi, M., Caballero, C., Mijangos, L. et al. From target analysis to suspect and non-target screening of endocrine-disrupting compounds in human urine. Anal Bioanal Chem 414, 6855–6869 (2022)
N. Lopez-Herguedas, B. González-Gaya, N. Castelblanco-Boyacá, A. Rico, N. Etxebarria, M. Olivares, A. Prieto, O. Zuloaga. Characterization of the contamination fingerprint of wastewater treatment plant effluents in the Henares River Basin (central Spain) based on target and suspect screening analysis. Science of The Total Environment 806, 151262 (2022)
Mariana F.T. Sá, Verónica Castro, Ana I. Gomes, Daniela F.S. Morais, Rui V.P.S. Silva Braga, Isabel Saraiva, Bianca M. Souza-Chaves, Minkyu Park, Victoria Fernández-Fernández, Rosario Rodil, Rosa Montes, José Benito Quintana, Vítor J.P. Vilar. Tracking pollutants in a municipal sewage network impairing the operation of a wastewater treatment plant. Science of The Total Environment 817, 152518 (2022)
Castro, V., Quintana, J.B., López-Vázquez, J. et al. Development and application of an in-house library and workflow for gas chromatography–electron ionization–accurate-mass/high-resolution mass spectrometry screening of environmental samples. Anal Bioanal Chem 414, 6327–6340 (2022)
Musatadi, M.; González-Gaya, B.; Irazola, M.; Prieto, A.; Etxebarria, N.; Olivares, M.; Zuloaga, O. Multi-Target Analysis and Suspect Screening of Xenobiotics in Milk by UHPLC-HRMS/MS. Separations 8, 14 (2021)

Millifluidic devices to run innovative sample treatments and bioassays


Ali Sahragard, Pakorn Varanusupakul, Manuel Miró, Nanomaterial decorated electrodes in flow-through electrochemical sensing of environmental pollutants: A critical review, Trends in Environmental Analytical Chemistry 29, e00208 (2023)
Sara R. Fernandes; Luisa Barreiros; Benedita Sampaio-Maia; Manuel Miró; Marcela A. Segundo, Total analysis system for the determination of uremic toxins in human plasma based on bead injection solid phase extraction hyphenated to mass spectrometry,  Analytica Chimica Acta 1277, 341668 (2023)
Ali Sahragard, Waleed Alahmad, Thidarat Samkumpim, Manuel Miró, Pakorn Varanusupakul, In-line gas purging exploiting a novel converging flow-on paper optosensing device for the determination of total ammonia-nitrogen in water samples, Advances in Sample Preparation 7, 1000766 (2023)
Llucia García-Moll, Alexandra Sixto, Enrique J. Carrasco-Correa, Manuel Miró, 3D-printed chemiluminescence flow cells with customized cross-section geometry for enhanced analytical performance, Talanta 255, 124211 (2023) 
M. Dvořák, M. Miró, P. Kubáň. Automated Sequential Injection-Capillary Electrophoresis for Dried Blood Spot Analysis: A Proof-of-Concept Study. Anal. Chem. 94, 5301–5309 (2022)
Carrasco-Correa, E.J., Herrero-Martínez, J.M., Simó-Alfonso, E.F. et al. 3D printed spinning cup-shaped device for immunoaffinity solid-phase extraction of diclofenac in wastewaters. Microchim Acta 189, 173 (2022)
Ali Sahragard, Pakorn Varanusupakul, Manuel Miró. Interfacing liquid-phase microextraction with electrochemical detection: A critical review. TrAC Trends in Analytical Chemistry 157, 116749 (2022)
Fernandes, S.R., Barreiros, L., Sá, P. et al. Automatic and renewable micro-solid-phase extraction based on bead injection lab-on-valve system for determination of tranexamic acid in urine by UHPLC coupled with tandem mass spectrometry. Anal Bioanal Chem 414, 649–659 (2022)
Ali Sahragard, Miloš Dvořák, Enrique J. Carrasco-Correa, Pakorn Varanasupakul, Pavel Kubáň, Manuel Miró. Programmable Millifluidic Platform Integrating Automatic Electromembrane Extraction Cleanup and In-Line Electrochemical Detection: A Proof of Concept. ACS Sens. 7, 3161–3168 (2022)
Llucia García-Moll, Alexandra Sixto, Enrique Javier Carrasco-Correa, Manuel Miró. 3D-printed chemiluminescence flow cells with customized cross-section geometry for enhanced analytical performance. Talanta 255, 124211 (2022)

Assess the effects of identified emerging contaminants in waters and strategies for mitigation


Presumido P.H., Ribeirinho-Soares S., Montes R., Quintana J.B., Rodil R., Ribeiro M., Neuparth T., Santos M.M., Feliciano M., Nunes O.C., Gomes A.I., Vilar V.J.P. Ozone membrane contactor for tertiary treatment of urban wastewater: Chemical, microbial and toxicological assessment, Science of the Total Environment, 892, 164492 (2023)
Montes R., Méndez S., Cobas J., Carro N., Neuparth T., Alves N., Santos M.M., Quintana J.B., Rodil R. Occurrence of persistent and mobile chemicals and other contaminants of emerging concern in Spanish and Portuguese wastewater treatment plants, transnational river basins and coastal water, Science of the Total Environment, 885, 163737 (2023)
Carro N., Cobas J., Otero A., Fernández R., García I., Ignacio M., Mouteira A.Spatial distribution and source identification of phthalates and organochlorine compounds in Galician mussels (NW Spain), Marine Pollution Bulletin, 194, 115393 (2023)
Amanda Cohen-Sánchez, Antonia Solomando, Samuel Pinya, Silvia Tejada, José M. Valencia, Antonio Box and Antoni Sureda, Microplastic presence in the digestive tract of pearly razorfish Xyrichtys novacula causes oxidative Stress in liver tissue, Toxics 11,  365 (2023)
S.M. Mendoza, M.P. García-Moll, V.H. Fernandez, M. Barrios, R. Mena, S. Miriuka, M. Cledon, Microplastics in stomach contents of juvenile Patagonian blennies (Eleginops maclovinus), Science of the Total Environment, 894, 164684 (2023)
Naroa Lopez-Herguedas, M. Irazola, Iker Alvarez-Mora, Gorka Orive, Unax Lertxundi, Maitane Olivares, Olatz Zuloaga, Ailette Prieto, Comprehensive micropollutant characterization of wastewater during Covid-19 crisis in 2020: Suspect screening and environmental risk prioritization strategy. Science of the Total Environment 873, 162281 (2023) 
Naroa Lopez-Herguedas, Leire Mijangos, Iker Alvarez-Mora, Belén González-Gaya, T. Uribe-Echeverria, Nestor Etxebarria, Olatz Zuloaga, Maitane Olivares, Ailette Prieto, Suspect screening of chemicals in hospital wastewaters using effect-directed analysis approach as prioritization strategy. Molecules 28, 1212 (2023)
Susana Barros, Nélson Alves, Marlene Pinheiro, Marta Ribeiro, Hugo Morais, Rosa Montes, Rosario Rodil, José Benito Quintana, Ana M. Coimbra, Miguel M. Santos, Teresa Neuparth. Are Fish Populations at Risk? Metformin Disrupts Zebrafish Development and Reproductive Processes at Chronic Environmentally Relevant Concentrations. Environ. Sci. Technol. 57, 1049–1059 (2023)
Naroa Lopez-Herguedas, Belén González-Gaya, Alicia Cano, Iker Alvarez-Mora, Leire Mijangos, Nestor Etxebarria, Olatz Zuloaga, Maitane Olivares, Ailette Prieto,Effect-directed analysis of a hospital effluent sample using A-YES for the identification of endocrine disrupting compounds. Science of The Total Environment 850, 157985 (2022)
Iker Alvarez-Mora, Valérie Bolliet, Naroa Lopez-Herguedas, Lyen Castro, Eneritz Anakabe, Mathilde Monperrus, Nestor Etxebarria. Prioritization based on risk assessment to study the bioconcentration and biotransformation of pharmaceuticals in glass eels (Anguilla anguilla) from the Adour estuary (Basque Country, France). Environmental Pollution 311, 120016 (2022)
Iker Alvarez-Mora, Leire Mijangos, Naroa Lopez-Herguedas, Jose M. Amigo, Harkaitz Eguiraun, Maddi Salvoch, Mathilde Monperrus, Nestor Etxebarria. SETApp: A machine learning and image analysis based application to automate the sea urchin embryo test. Ecotoxicology and Environmental Safety 241, 113728 (2022)
Carro, N., García I., Ignacio. M., Mouteira, A., Cobas, J. Spatial and temporal variability of organochlorine compounds in wild mussels from Galician Rías (2010-2019), Environmental Advances, 9, 100258 (2022)
Sá M.F.T., Castro V., Gomes A.I., Morais D.F.S., Silva Braga R.V.P.S., Saraiva I., Souza-Chaves B.M., Park M., Fernández-Fernández V., Rodil R., Montes R., Quintana J.B., Vilar V.J.P. Tracking pollutants in a municipal sewage network impairing the operation of a wastewater treatment plant, Science of the Total Environment, 817, 152518 (2022)
Presumido P.H., Montes R., Quintana J.B., Rodil R., Feliciano M., Puma G.L., Gomes A.I., Vilar V.J.P. Ozone membrane contactor to intensify gas/liquid mass transfer and contaminants of emerging concern oxidation, Journal of Environmental Chemical Engineering, 10 (6), 108671 (2022)
Susana Barros, Marta Ribeiro, Ana M. Coimbra, Marlene Pinheiro, Hugo Morais, Nélson Alves, Rosa Montes, Rosario Rodil, José Benito Quintana, Miguel M. Santos, Teresa Neuparth. Metformin disrupts Danio rerio metabolism at environmentally relevant concentrations: A full life-cycle study. Science of The Total Environment 846, 157361 (2022)
T. Neuparth, N. Alves, A.M. Machado, M. Pinheiro, R. Montes, R. Rodil, S. Barros, R. Ruivo, L.Filipe C. Castro, J.B. Quintana, M.M. Santos. Neuroendocrine pathways at risk? Simvastatin induces inter and transgenerational disruption in the keystone amphipod Gammarus locusta. Aquatic Toxicology 244, 106095 (2022)
Benigno José Sieira, Rosario Rodil, Rafael Cela, José Benito Quintana, Rosa Montes. Transformation products of the high-volume production chemicals 1-vinyl-2-pyrrolidinone and 2-piperazin-1-ylethanamine formed by UV photolysis. Chemosphere 287, 132394 (2022)

Estimate the bioaccessible and bioavailable fractions of emerging contaminants


Maria Pau Garcia-Moll, Llucia Garcia-Moll, Enrique Javier Carrasco-Correa, Miquel Oliver, Ernesto F. Simo-Alfonso, and Manuel Miró, Biomimetic Dispersive Solid-Phase Microextraction: A Novel Concept for High-Throughput Estimation of Human Oral Absorption of Organic Compounds, Analytical Chemistry 95, 13123-13131 (2023)
Lais A. Souza, Rodrigo M.A. Pedreira, Manuel Miró, Vanessa Hatje. Evidence of high bioaccessibility of gadolinium-contrast agents in natural waters after human oral uptake. Science of The Total Environment 793, 148506 (2021)
Enrique Javier Carrasco-Correa, Julia Ruiz-Allica, Juan Francisco Rodríguez-Fernández, Manuel Miró. Human artificial membranes in (bio)analytical science: Potential for in vitro prediction of intestinal absorption-A review. TrAC Trends in Analytical Chemistry 145, 116446 (2021)
Javier López-Vázquez, Rosario Rodil, María J. Trujillo-Rodríguez, José Benito Quintana, Rafael Cela, Manuel Miró. Mimicking human ingestion of microplastics: Oral bioaccessibility tests of bisphenol A and phthalate esters under fed and fasted states. Science of The Total Environment 826, 154027 (2022)

Upgrade millifluidic devices to run innovative in-vitro bioassays


Margherita Izzi, Miquel Oliver, Helena Mateos, Gerardo Palazzo, Nicola Cioffi and Manuel Miró, Analytical probing of membranotropic effects of antimicrobial copper nanoparticles on lipid vesicles as membrane models, Nanoscale Advances 5, 6533-6541 (2023)
Maite V. Aguinaga Martínez, Natali Jozičová, Jan Dušek, Burkhard Horstkotte, Petr Pávek, Manuel Miró, Hana Sklenářová. Real-time monitoring of Metridia luciferase release from cells upon interaction with model toxic substances by a fully automatic flow setup – A proof of concept. Talanta 245, 123465 (2022)

Study the relationships between certain diseases with the exposure to emerging contaminants


Assess the exposure to contaminants through urine analysis and wastewater-based epidemiology


Senta I., Krizman-Matasic I., Kostanjevecki P., Gonzalez-Mariño I., Rodil R., Quintana J.B., Mikac I., Terzic S., Ahel M. Assessing the impact of a major electronic music festival on the consumption patterns of illicit and licit psychoactive substances in a Mediterranean city using wastewater analysis, Science of the Total Environment, 892, 164547 (2023)
Andrea Estévez-Danta, Lubertus Bijlsma, Ricardo Capela, Rafael Cela, Alberto Celma, Félix Hernández, Unax Lertxundi, João Matias, Rosa Montes, Gorka Orive, Ailette Prieto, Miguel M. Santos, Rosario Rodil, José Benito Quintana. Use of illicit drugs, alcohol and tobacco in Spain and Portugal during the COVID-19 crisis in 2020 as measured by wastewater-based epidemiology. Science of The Total Environment 836, 155697 (2022)
Andrea Estévez-Danta, Rosa Montes, Lubertus Bijlsma, Rafael Cela, Alberto Celma, Iria González-Mariño, Manuel Miró, Vanessa Gutmann, Unai Pérez de San Román-Landa, Ailette Prieto, Mireia Ventura, Rosario Rodil, José Benito Quintana. Source identification of amphetamine-like stimulants in Spanish wastewater through enantiomeric profiling. Water Research 206, 117719 (2021)
Andrea Estévez-Danta, Lubertus Bijlsma, Ricardo Capela, Rafael Cela, Alberto Celma, Félix Hernández, Unax Lertxundi, João Matias, Rosa Montes, Gorka Orive, Ailette Prieto, Miguel M. Santos, Rosario Rodil, José Benito Quintana. Use of illicit drugs, alcohol and tobacco in Spain and Portugal during the COVID-19 crisis in 2020 as measured by wastewater-based epidemiology. Science of The Total Environment 836, 155697 (2022)
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